| The Synthesis of Metal Complexes with Macrocyclic Glyoxime Ether Contributor(s): Karapinar Emin (Author) |
|
 |
ISBN: 3659427292 ISBN-13: 9783659427299 Publisher: LAP Lambert Academic Publishing OUR PRICE: $33.75 Product Type: Paperback Published: July 2013 |
| Additional Information |
| BISAC Categories: - Science | Chemistry - Inorganic |
| Physical Information: 0.23" H x 6" W x 9" (0.33 lbs) 96 pages |
| Descriptions, Reviews, Etc. |
| Publisher Description: In this work, by the reaction of four different chloroglyoximes with 4'-Amminobenzo 15-Crown-5] in absolute ethanol, eight of new macrocylic glyoxime ether compounds and their Ni(II), Co(II) and Cu(II) complexes have been synthesized. For this, firstly chlorophenylglyoxime, p-tolylchloroglyoxime, p-chlorophenyl chloroglyoxime and 4'-biphenylchloroglyoxime were synthesized according to previously reported literatures. Then novel glyoxime derivatives with macrocyclic glyoxime ethers by the reactions between these compounds with 4'-amminobenzo 15-crown-5] were obtained. The complexes of these ligands with metal chlorid salts have been formed. Finally, the UV-VIS, IR, AAS and 1H NMR spectroscopic properties of these compounds were investigated and clarified by the help of the results of elemental analyses and the spectroscopic methods. The content of this book is based on an experimental study for my Ph.D thesis submitted to Selcuk University, Konya, Turkey in 2002. |